Use of a new type of 8-hydroxyquinoline-5-sulphonic acid cellulose (sulphoxine cellulose) for the preconcentration of trace metals from highly mineralised water prior their GFAAS determination

K. Zih-Perényi, A. Lásztity, Zs Horváth, Á Lévai

Research output: Contribution to journalArticle

76 Citations (Scopus)

Abstract

Sulphoxine cellulose microcolumn was used in an FI-GFAAS system for the preconcentration of trace metals, Cd, Co, Ni, Pb and V from water and from highly mineralised water and also in the presence of complexing agent, e.g. citrate. The recovery was quantitative at pH 5 for all of the elements from NIST 1643c trace elements in water SRM and from highly mineralised water samples. No significant difference was found in the sorption of V(IV) and V(V) during preconcentration. The preparation of the 8-hydroxyquinoline-5- sulphonic acid cellulose (sulphoxine-cellulose) by Mannich reaction from aminoethyl cellulose or via chlorodeoxy and ethylenediamine Cellulose is also described.

Original languageEnglish
Pages (from-to)673-679
Number of pages7
JournalTalanta
Volume47
Issue number3
DOIs
Publication statusPublished - Nov 1998

Keywords

  • GFAAS determination
  • Sulphoxine cellulose
  • Trace metals

ASJC Scopus subject areas

  • Analytical Chemistry

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