Synthesis and characterisation of alkaline earth-iron(III) double hydroxides

Mónika Sipiczki, Dávid F. Srankó, Ákos Kukovecz, Zoltán Kónya, Pál Sipos, István Pálinkó

Research output: Contribution to journalArticle

9 Citations (Scopus)

Abstract

Double hydroxides containing alkaline earth and iron(III) ions were synthesised by the coprecipitation method. The solid materials obtained were characterised by a range of instrumental methods (powder X-ray diffractometry, thermogravimetry, scanning electron microscopy, energy dispersive X-ray fluorescence spectrometry, elemental maps, and infrared spectroscopy). It was found that the Ca(II)Fe(III), Mg(II)Fe(III), and Ba(II)Fe(III) double hydroxides had layered structures, while Sr(II)Fe(III) had not. The optimum conditions for synthesis of Ca(II)Fe(III)-layered double hydroxides (materials to be used in further studies) were also elaborated.

Original languageEnglish
Pages (from-to)840-846
Number of pages7
JournalChemical Papers
Volume65
Issue number6
DOIs
Publication statusPublished - Dec 1 2011

Keywords

  • Alkaline earth-iron(III) double hydroxides
  • Characterisation
  • Instrumental methods
  • Synthesis
  • Synthesis optimisation

ASJC Scopus subject areas

  • Biochemistry
  • Chemistry(all)
  • Chemical Engineering(all)
  • Industrial and Manufacturing Engineering
  • Materials Chemistry

Fingerprint Dive into the research topics of 'Synthesis and characterisation of alkaline earth-iron(III) double hydroxides'. Together they form a unique fingerprint.

  • Cite this