Synthesis and characterisation of alkaline earth-iron(III) double hydroxides

Mónika Sipiczki, Dávid F. Srankó, Á. Kukovecz, Z. Kónya, P. Sipos, I. Pálinkó

Research output: Contribution to journalArticle

9 Citations (Scopus)

Abstract

Double hydroxides containing alkaline earth and iron(III) ions were synthesised by the coprecipitation method. The solid materials obtained were characterised by a range of instrumental methods (powder X-ray diffractometry, thermogravimetry, scanning electron microscopy, energy dispersive X-ray fluorescence spectrometry, elemental maps, and infrared spectroscopy). It was found that the Ca(II)Fe(III), Mg(II)Fe(III), and Ba(II)Fe(III) double hydroxides had layered structures, while Sr(II)Fe(III) had not. The optimum conditions for synthesis of Ca(II)Fe(III)-layered double hydroxides (materials to be used in further studies) were also elaborated.

Original languageEnglish
Pages (from-to)840-846
Number of pages7
JournalChemical Papers
Volume65
Issue number6
DOIs
Publication statusPublished - Dec 2011

Fingerprint

Hydroxides
Iron
Earth (planet)
Coprecipitation
Thermogravimetry
X ray powder diffraction
X ray diffraction analysis
X-Ray Emission Spectrometry
Thermogravimetric analysis
Infrared spectroscopy
Electron Scanning Microscopy
Powders
Scanning electron microscopy
Spectrum Analysis
Ions
X-Rays
ferric hydroxide

Keywords

  • Alkaline earth-iron(III) double hydroxides
  • Characterisation
  • Instrumental methods
  • Synthesis
  • Synthesis optimisation

ASJC Scopus subject areas

  • Chemistry(all)
  • Chemical Engineering(all)
  • Biochemistry
  • Industrial and Manufacturing Engineering
  • Materials Chemistry

Cite this

Synthesis and characterisation of alkaline earth-iron(III) double hydroxides. / Sipiczki, Mónika; Srankó, Dávid F.; Kukovecz, Á.; Kónya, Z.; Sipos, P.; Pálinkó, I.

In: Chemical Papers, Vol. 65, No. 6, 12.2011, p. 840-846.

Research output: Contribution to journalArticle

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AU - Kukovecz, Á.

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AU - Sipos, P.

AU - Pálinkó, I.

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