Semi-real-time acquisition for fast pure shift NMR at maximum resolution

P. Király, Mathias Nilsson, Gareth A. Morris

Research output: Contribution to journalArticle

4 Citations (Scopus)

Abstract

Homonuclear decoupling can give impressive improvements in spectral resolution when overlapping multiplet structures limit the interpretability of NMR spectra. General homodecoupling methods (“pure shift NMR”) typically use either interferogram-style acquisition, which is slow but gives optimum resolution, or real-time acquisition, which is fast but gives broader lines. Here we describe an alternative data acquisition strategy that allows rapid acquisition without resolution loss, illustrating the method with band-selective homodecoupling experiments and demonstrating its advantages over competing methods.

Original languageEnglish
Pages (from-to)19-27
Number of pages9
JournalJournal of Magnetic Resonance
Volume293
DOIs
Publication statusPublished - Aug 1 2018

Keywords

  • Band-selective decoupling
  • Homodecoupling
  • NMR
  • Pure shift NMR

ASJC Scopus subject areas

  • Biophysics
  • Biochemistry
  • Nuclear and High Energy Physics
  • Condensed Matter Physics

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