Reversed-phase foam chromatography. Separation of palladium, bismuth and nickel in the tributyl phosphate-thiourea-perchloricacid system

T. Braun, A. B. Farag

Research output: Contribution to journalArticle

54 Citations (Scopus)

Abstract

The feasibility of using TBP-loaded polyurethane foams as column fillings in reversed-phase chromatography was examined and their capacities were determined. Separation of nickel, bismuth, and palladium was achieved. The effect of flow-rate, temperature and ratio of the separated ions on the efficiency of separation was tested. Elution with high flow-rate affected the efficiency of the column at 25° but not at higher temperature (e.g. 35°). Once the column was prepared, it could be used several times without affecting its efficiency.

Original languageEnglish
Pages (from-to)265-276
Number of pages12
JournalAnalytica Chimica Acta
Volume61
Issue number2
DOIs
Publication statusPublished - Sep 1972

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ASJC Scopus subject areas

  • Analytical Chemistry
  • Biochemistry
  • Environmental Chemistry
  • Spectroscopy

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