Rapid method for combined X—{1H} NOE and T1 measurement using heteronuclear polarization transfer

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Abstract

A polarization transfer enhanced inversion‐recovery experiment is proposed for the combined measurement of heteronuclear T1 and NOE of low‐γ nuclei. This method offers significant time savings compared with conventional relaxation measurements. The reliability and accuracy of the combined T1, and NOE determination and its dependence on the experimental set‐up is also demonstrated. The proposed approach may be preferred for multiple field/multiple temperature model‐free analysis of molecular dynamics.

Original languageEnglish
Pages (from-to)871-873
Number of pages3
JournalMagnetic Resonance in Chemistry
Volume33
Issue number11
DOIs
Publication statusPublished - 1995

Keywords

  • heteronuclear T and NOE
  • INEPT
  • inversion‐recovery

ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)

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