Optical resolution of 2-(3-chloro-phenyl)-3,4A, 5,6,7,7A- hexahydrocyclopentapyrimidin-4-one with O,O'-dibenzoyl-2R,3R-tartaric acid in water-chloroform two phase solvent system

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Abstract

Optical resolution of racemic 2-(3-chloro-phenyl)-3,4a,5,6,7,7a- hexahydrocyclopentapyrimidin-4-one with O,O'-dibenzoyl-2R,3R-tartaric acid in an unusual solvent combination, in water-chloroform two phase solvent system was accomplished. During enantiomeric enrichment of the resulted raw base the optically active base can be recovered from the ethanolic mother liquor.

Original languageEnglish
Pages (from-to)2265-2270
Number of pages6
JournalSynthetic Communications
Volume29
Issue number13
DOIs
Publication statusPublished - Jan 1 1999

ASJC Scopus subject areas

  • Organic Chemistry

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