Novel synthesis and crystal structure of 1,4-bis(3-chloro-1,1,3-trimethylbutyl)benzene

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Abstract

A symmetrical isobutene adduct was synthesized with high yield at -80 °C by means of the 1,4-bis(1-chloro-1-methylethyl)benzene/isobutene system using tetrabutylammonium chloride. The main product under the reaction conditions applied was the symmetrical isobutene adduct, which was crystallized from a hexane/dichloromethane solution and the crystals were analyzed by X-ray crystallography.

Original languageEnglish
Pages (from-to)810-811
Number of pages2
JournalChemistry Letters
Issue number7
Publication statusPublished - 2000

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Benzene
Crystal structure
Methylene Chloride
X ray crystallography
Hexanes
Crystals
isobutylene

ASJC Scopus subject areas

  • Chemistry(all)

Cite this

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title = "Novel synthesis and crystal structure of 1,4-bis(3-chloro-1,1,3-trimethylbutyl)benzene",
abstract = "A symmetrical isobutene adduct was synthesized with high yield at -80 °C by means of the 1,4-bis(1-chloro-1-methylethyl)benzene/isobutene system using tetrabutylammonium chloride. The main product under the reaction conditions applied was the symmetrical isobutene adduct, which was crystallized from a hexane/dichloromethane solution and the crystals were analyzed by X-ray crystallography.",
author = "S. K{\'e}ki and G. De{\'a}k and A. B{\'e}nyei and M. Zsuga",
year = "2000",
language = "English",
pages = "810--811",
journal = "Chemistry Letters",
issn = "0366-7022",
publisher = "Chemical Society of Japan",
number = "7",

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T1 - Novel synthesis and crystal structure of 1,4-bis(3-chloro-1,1,3-trimethylbutyl)benzene

AU - Kéki, S.

AU - Deák, G.

AU - Bényei, A.

AU - Zsuga, M.

PY - 2000

Y1 - 2000

N2 - A symmetrical isobutene adduct was synthesized with high yield at -80 °C by means of the 1,4-bis(1-chloro-1-methylethyl)benzene/isobutene system using tetrabutylammonium chloride. The main product under the reaction conditions applied was the symmetrical isobutene adduct, which was crystallized from a hexane/dichloromethane solution and the crystals were analyzed by X-ray crystallography.

AB - A symmetrical isobutene adduct was synthesized with high yield at -80 °C by means of the 1,4-bis(1-chloro-1-methylethyl)benzene/isobutene system using tetrabutylammonium chloride. The main product under the reaction conditions applied was the symmetrical isobutene adduct, which was crystallized from a hexane/dichloromethane solution and the crystals were analyzed by X-ray crystallography.

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M3 - Article

SP - 810

EP - 811

JO - Chemistry Letters

JF - Chemistry Letters

SN - 0366-7022

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