Nitrogen bridgehead compounds 871. Synthesis of 3-azarutecarpine (14-azanauclefine) and its 7-methyl derivative

I. Hermecz, J. Kökösi, Benjamin Podányi, Zsuzsanna Liko

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Abstract

3-Azarutecarpine (14-azanauclefine) derivatives 2 were prepared by Fischer indolization of 6-phenylhydrazono-6,7,8,9-tetrahydro-11H-dipyrido[1,2-a;4,3-d]pyrimidine-11-ones 8. Compounds 8 were obtained from 6,7,8,9-tetrahydro-11H-dipyrido-[1,2-a;4,3-d]pyrimidinones 7 with phenyldiazonium chloride. New compounds are characterized by UV, IR, 1H and 13C NMR spectroscopy.

Original languageEnglish
Pages (from-to)7789-7796
Number of pages8
JournalTetrahedron
Volume52
Issue number22
DOIs
Publication statusPublished - May 27 1996

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Pyrimidinones
Nitrogen Compounds
Nuclear magnetic resonance spectroscopy
Chlorides
Magnetic Resonance Spectroscopy
Derivatives
pyrimidine
Proton Magnetic Resonance Spectroscopy
Carbon-13 Magnetic Resonance Spectroscopy

ASJC Scopus subject areas

  • Biochemistry
  • Organic Chemistry
  • Drug Discovery

Cite this

Nitrogen bridgehead compounds 871. Synthesis of 3-azarutecarpine (14-azanauclefine) and its 7-methyl derivative. / Hermecz, I.; Kökösi, J.; Podányi, Benjamin; Liko, Zsuzsanna.

In: Tetrahedron, Vol. 52, No. 22, 27.05.1996, p. 7789-7796.

Research output: Contribution to journalArticle

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