Mossbauer and X-ray diffraction study of isothermal ageing effect at 500 °C in electrochemically deposited Fe-Ni-Cr alloys

E. Kuzmann, M. R. El-Sharif, C. U. Chisholm, A. Vértes

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

Mossbauer spectroscopy, X-ray diffractometry and microprobe analysis were used to study electrodeposited Fe-Ni-Cr (40-50% Fe, 40-47% Ni, 3-5% Cr) alloys isothermally aged at 500°C from 5 minutes to 100 hours in an inert argon gas atmosphere. The main phase of the as-deposited samples exhibits ferromagnetic microcrystalline behavior, whereas the thermally prepared samples of same composition are always paramagnetic. The dominant effect of ageing is an oxidation process which resulted in the formation of hematite and magnetite iron oxides in considerable amounts and which are attributable to the presence of oxygen inclusions in the as-electrodeposited samples.

Original languageEnglish
Pages (from-to)789-792
Number of pages4
JournalJournal of Radioanalytical and Nuclear Chemistry
Volume240
Issue number3
DOIs
Publication statusPublished - 1999

Fingerprint

Hematite
Mossbauer spectroscopy
Magnetite
Iron oxides
X-Ray Diffraction
X ray diffraction analysis
Argon
Aging of materials
Mossbauer Spectroscopy
Ferrosoferric Oxide
Noble Gases
X ray diffraction
Oxidation
Oxygen
Chemical analysis
Atmosphere
Gases
X-Rays
ferric oxide

ASJC Scopus subject areas

  • Analytical Chemistry
  • Inorganic Chemistry
  • Nuclear Energy and Engineering

Cite this

Mossbauer and X-ray diffraction study of isothermal ageing effect at 500 °C in electrochemically deposited Fe-Ni-Cr alloys. / Kuzmann, E.; El-Sharif, M. R.; Chisholm, C. U.; Vértes, A.

In: Journal of Radioanalytical and Nuclear Chemistry, Vol. 240, No. 3, 1999, p. 789-792.

Research output: Contribution to journalArticle

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