Measuring couplings in crowded NMR spectra

Pure shift NMR with multiplet analysis

M. Foroozandeh, R. W. Adams, P. Király, M. Nilsson, G. A. Morris

Research output: Contribution to journalArticle

43 Citations (Scopus)

Abstract

The PSYCHE method for pure shift NMR is exploited to generate 2D J spectra with full decoupling in one dimension and multiplet structure in the other, allowing spin-spin coupling constants to be measured even in very crowded spectra. Significant improvements over existing techniques are demonstrated for the hormones estradiol and androstenedione.

Original languageEnglish
Pages (from-to)15410-15413
Number of pages4
JournalChemical Communications
Volume51
Issue number84
DOIs
Publication statusPublished - 2015

Fingerprint

Androstenedione
Hormones
Estradiol
Nuclear magnetic resonance

ASJC Scopus subject areas

  • Chemistry(all)
  • Catalysis
  • Ceramics and Composites
  • Electronic, Optical and Magnetic Materials
  • Surfaces, Coatings and Films
  • Materials Chemistry
  • Metals and Alloys

Cite this

Measuring couplings in crowded NMR spectra : Pure shift NMR with multiplet analysis. / Foroozandeh, M.; Adams, R. W.; Király, P.; Nilsson, M.; Morris, G. A.

In: Chemical Communications, Vol. 51, No. 84, 2015, p. 15410-15413.

Research output: Contribution to journalArticle

Foroozandeh, M. ; Adams, R. W. ; Király, P. ; Nilsson, M. ; Morris, G. A. / Measuring couplings in crowded NMR spectra : Pure shift NMR with multiplet analysis. In: Chemical Communications. 2015 ; Vol. 51, No. 84. pp. 15410-15413.
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