Isolation of 5α and 5β-dihydrorubrosterone from Silene otites L. (Wib)

M. Báthori, J. P. Girault, I. Máthé, R. Lafont

Research output: Contribution to journalArticle

8 Citations (Scopus)

Abstract

5α-Dihydrorubrosterone (2β, 3β, 14α, 17β-tetrahydroxy-5α-androst-7-ene-6-one), a new 19-carbon 5α-ecdysteriod, was isolated together with its 5β counterpart from the aerial parts of Silene otites L. (Wib.) (Caryophyllaceae) by a combination of solvent partition, low-pressure column chromatography, thin-layer chromatography (normal-phase and reversed-phase) and finally HPLC. Mass spectrometry and nuclear magnetic resonance spectroscopic procedures were used for compound characterization. Copyright (C) 2000 John Wiley and Sons, Ltd.

Original languageEnglish
Pages (from-to)464-467
Number of pages4
JournalBiomedical Chromatography
Volume14
Issue number7
DOIs
Publication statusPublished - 2000

Fingerprint

Caryophyllaceae
Silene
Thin layer chromatography
Column chromatography
Thin Layer Chromatography
Mass spectrometry
Chromatography
Mass Spectrometry
Magnetic Resonance Spectroscopy
Carbon
High Pressure Liquid Chromatography
Nuclear magnetic resonance
Antennas
Pressure
5-dihydrorubrosterone

ASJC Scopus subject areas

  • Analytical Chemistry
  • Clinical Biochemistry
  • Biochemistry, Genetics and Molecular Biology(all)
  • Biochemistry
  • Pharmacology

Cite this

Isolation of 5α and 5β-dihydrorubrosterone from Silene otites L. (Wib). / Báthori, M.; Girault, J. P.; Máthé, I.; Lafont, R.

In: Biomedical Chromatography, Vol. 14, No. 7, 2000, p. 464-467.

Research output: Contribution to journalArticle

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