High-speed tracking of fast chemical precipitations

Réka Zahorán, Á. Kukovecz, A. Tóth, D. Horváth, Gábor Schuszter

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Abstract

Heterogeneous reactions taking place in the aqueous phase bear significant importance both in applied and fundamental research. Among others, producing solid catalysts, crystallizing biomorphs or pharmaceutically relevant polymorphs, and yielding bottom-up synthesised precipitate structures are prominent examples. To achieve a better control on product properties, reaction kinetics and mechanisms must be taken into account especially in dynamic systems where transport processes are coupled to chemistry. Since the characteristic time scale of numerous precipitation reactions falls below 1 s within the relevant concentration range, unique experimental protocols are needed. Herein we present a high-speed camera supported experimental procedure capable of determining such characteristic time scales in the range of 10 ms to 1 s. The method is validated both experimentally and by performing 3D hydrodynamic simulations.

Original languageEnglish
Pages (from-to)11345-11350
Number of pages6
JournalPhysical Chemistry Chemical Physics
Volume21
Issue number21
DOIs
Publication statusPublished - Jan 1 2019

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ASJC Scopus subject areas

  • Physics and Astronomy(all)
  • Physical and Theoretical Chemistry

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