High-field NMR studies of 3β-tetrahydropyranyloxy steroids

Zsuzsanna Szendi, P. Forgó, K. Kövér, Frederick Sweet

Research output: Contribution to journalArticle

3 Citations (Scopus)

Abstract

Comprehensive NMR studies were carried out on 3β-hydroxy-pregnene and cholestene analogs, each containing a tetrahydropyranyl ether group at the 3-position. Two-dimensional NMR experiments (COSY, TOCSY, HSQC, and HSQC-TOCSY) permitted the complete assignments of both the 1H and 13C resonances of these derivatives in deuterated benzene or chloroform. The aromatic solvent-induced NMR signal shifts (ASIS) were also investigated. Copyright (C) 2000 Elsevier Science Inc.

Original languageEnglish
Pages (from-to)415-422
Number of pages8
JournalSteroids
Volume65
Issue number7
DOIs
Publication statusPublished - Jul 2000

Fingerprint

Pregnenes
Chloroform
Benzene
Ether
Steroids
Nuclear magnetic resonance
Derivatives
Experiments

Keywords

  • Steroids
  • Tetrahydropyranyl ethers
  • Two-dimensional NMR spectroscopy

ASJC Scopus subject areas

  • Biochemistry
  • Endocrinology
  • Molecular Biology

Cite this

High-field NMR studies of 3β-tetrahydropyranyloxy steroids. / Szendi, Zsuzsanna; Forgó, P.; Kövér, K.; Sweet, Frederick.

In: Steroids, Vol. 65, No. 7, 07.2000, p. 415-422.

Research output: Contribution to journalArticle

Szendi, Zsuzsanna ; Forgó, P. ; Kövér, K. ; Sweet, Frederick. / High-field NMR studies of 3β-tetrahydropyranyloxy steroids. In: Steroids. 2000 ; Vol. 65, No. 7. pp. 415-422.
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