Heterocyclic compounds from sugars. XIV—Structure determination and conformational analysis of the four diastereoisomeric methyl 3‐Acetyl‐5,5‐dimethyl‐2‐(D‐galacto‐pentaacetoxypentyl)‐1,3‐thiazolidine‐4‐carboxylate 1‐Oxides

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Abstract

1H and 13C NMR experiments were performed to analyse the conformation and stereochemistry of diastereomeric sulphoxides of 1,3‐thiazolidine derivatives. The conformation of the thiazolidine ring was verified by an NOE study. ASIS and 13C chemical shift data supported the sulphoxide configuration.

Original languageEnglish
Pages (from-to)137-142
Number of pages6
JournalMagnetic Resonance in Chemistry
Volume30
Issue number2
DOIs
Publication statusPublished - 1992

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Keywords

  • C chemical shifts
  • 1,3‐Thiazolidine ring conformation
  • ASIS
  • NOE
  • Sulphoxide configuration

ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)

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