Comparison of powder and single crystal data of C60(C14H10O2), an oxygen containing anthracene derivative of C60

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Abstract

C60(C14H10O2), an anthracene derivative of C60 was successfully synthesized yielding both polycrystalline and single crystal samples. These were investigated by x-ray diffraction methods, synchrotron radiation was utilized in powder and conventional x-ray source in single crystal studies. The molecular and crystal structure of C60(C14H10O2) was determined from single crystal measurements revealing the incorporation of two oxygen atoms into the middle benzene ring of anthracene. Parallel beam powder data fully supports the structure, however, it does not provide sufficient information for unconstrained structure refinement.

Original languageEnglish
Pages (from-to)879-884
Number of pages6
JournalMaterials Science Forum
Volume228-231
Issue numberPART 2
Publication statusPublished - Dec 1 1996

Keywords

  • Addition Reaction
  • Anthracene
  • Fullerenes
  • Powder Diffraction
  • Single Crystal Diffraction
  • Structure Determination
  • Structure Refinement

ASJC Scopus subject areas

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

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